反应详情

0.2 mole (38.4 g) of 2,6-dichloronitrobenzene and 0.6 mole (54.6 g) of 3-aminopropane-1,2-diol in 200 ml of 1-methyl-2-pyrrolidone are heated to 80° C. The reaction mixture is diluted with ice. The product expected precipitates. After recrystallizing from isopropanol, it melts at 126° C.

1. additionThe reaction mixture is diluted with ice
2. customThe product expected precipitates
3. customAfter recrystallizing from isopropanol, it melts at 126° C.