反应详情

S-(2,4,5-Trichlorophenyl) 4-(acetoxy)thiobenzoate (10 g) in tetrahydrofuran was treated with 25 ml of 5.6M hydrochloric acid and stirred at room temperature overnight. The solvents were evaporated in vacuo to give a product which was purified by column chromatography (silica; ethyl acetate-hexane mixtures as eluant) to afford the title compound (5.4 g).

1. customThe solvents were evaporated in vacuo
2. customto give a product which
3. customwas purified by column chromatography (silica; ethyl acetate-hexane mixtures as eluant)