反应详情

Methyl bromoacetate (57 ul) was added to a mixture of the product from step (v) (0.2 g) and K2CO3 (0.251 g) in DMF (10 ml) and the mixture stirred at rt for 24 h. The mixture was partitioned between EtOAc/water, the organics separated, dried and evaporated under reduced pressure. The residue was purified by RPHPLC to afford the title compound, 0.057 g

1. customThe mixture was partitioned between EtOAc/water
2. customthe organics separated, dried
3. customevaporated under reduced pressure
4. customThe residue was purified by RPHPLC