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HRID2391703

反应详情

EQUATION

反应方程式

HRID 2391703 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：FC(F)Oc1ccccc1CBr
HCID2736998

2-(Difluoromethoxy)benzyl bromide

C8H7BrF2O

结构：COC(=O)c1sc(-n2cnc3cnccc32)cc1O
HCID68766294

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1sc(-n2cnc3cnccc32)cc1OCc1ccccc1OC(F)F
HCID68766710

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

In a similar manner as described for example B18, 207.7 mg of 2-(difluoromethoxy)benzyl bromide, 200 mg of methyl 3-hydroxy-5-(1H-imidazo[4,5-c]pyridin-1-yl)thiophene-2-carboxylate, 110.9 mg of potassium carbonate in 6 ml anhydrous DMF yield the title compound.