反应详情

To a solution of cyanophenol (25 g) and potassium carbonate (50 g) in 2-butanone (320 ml) was added bromooctane (61 ml) at room temperature. The stirred mixture was heated under reflux until TLC revealed complete reaction, i.e. about 48 hr. The mixture was filtered, after which the solvent and excess alkyl bromide were removed in vacuo to give a colorless liquid.

1. temperatureThe stirred mixture was heated
2. temperatureunder reflux until TLC
3. customreaction, i.e. about 48 hr
4. filtrationThe mixture was filtered
5. customafter which the solvent and excess alkyl bromide were removed in vacuo
6. customto give a colorless liquid