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HRID241029

反应详情

EQUATION

反应方程式

HRID 241029 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：CC(C)COC(=O)Cl
HCID62365

Isobutyl chloroformate

C5H9ClO2

结构：Nc1ccc(Br)c(F)c1N
HCID2783203

4-bromo-3-fluorobenzene-1,2-diamine

C6H6BrFN2

PRODUCTS

生成物

1
结构：Cc1nc2c(F)c(Br)ccc2n1C(=O)OCC(C)C
HCID68777136

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Synthesized according to the method of reagent preparation 19 using 5 4-bromo-3-fluorobenzene-1,2-diamine and acetylation with acetic anhydride in tetrahydrofurane in step 1 then treatment with isobutyl chloroformate in step 3. MS (EI) for C13H14BrN2O2: 328, 330 (MH+, Br isotope pattern).

WORKUP

后处理

  1. customSynthesized