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HRID2416132

反应详情

EQUATION

反应方程式

HRID 2416132 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)Cl)cc1
HCID7397

p-Toluenesulfonyl chloride

C7H7ClO2S

结构：N#Cc1ccc(-c2ccc3oc(CCO)cc3c2)cc1
HCID11482439

4-[2-(2-Hydroxyethyl)-1-benzofuran-5-yl]benzonitrile

C17H13NO2

PRODUCTS

生成物

1
结构：Cc1ccc(S(=O)(=O)OCCc2cc3cc(-c4ccc(C#N)cc4)ccc3o2)cc1
HCID11711405

2-[5-(4-cyanophenyl)-1-benzofuran-2-yl]ethyl 4-methylbenzenesulfonate

C24H19NO4S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

reacting 4-[2-(2-hyd roxyethyl)-1-benzofuran-5-yl]benzonitrile with para-toluenesulfonyl chloride and N,N-dimethylaminopyridine, in the presence of a base, such as triethylamine, to provide 2-[5-(4-cyanophenyl)-1-benzofuran-2-yl]ethyl 4-methylbenzenesulfonate; and