HRID250580

反应详情

EQUATION

反应方程式

HRID 250580 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To 5-isopropenyl-1H-pyrrolo[2,3-b]pyridine (98, 0.080 g, 0.501 mmol) in tetrahydrofuran (5.0 mL) was added 20% palladium hydroxide on carbon (5.0 mg). The reaction was stirred under hydrogen at 40 psi for 30 minutes. The reaction mixture was filtered and concentrated to give the compound (99, 0.078 g, 96%). MS (ESI) [M+H+]+=161.

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered
  2. concentrationconcentrated
  3. customto give the compound (99, 0.078 g, 96%)