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HRID25235

反应详情

EQUATION

反应方程式

HRID 25235 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CCOC(=O)c1ccc(N2CCC(NC(=O)OC(C)(C)C)CC2)nc1
HCID22574446

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1ccc(N2CCC(N)CC2)nc1
HCID11402429

3-Pyridinecarboxylic acid, 6-(4-amino-1-piperidinyl)-, ethyl ester

C13H19N3O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

2 次

PROCEDURE

实验过程

The product of stage b) is dissolved in ethyl acetate, a 3N solution of hydrochloric acid in ethyl acetate is added and the mixture is left stirring at ambient temperature for 10 hours. The product is filtered off and washed with acetone. The title product is obtained. M.p.: 148-150° C.

WORKUP

后处理

  1. waitthe mixture is left
  2. filtrationThe product is filtered off
  3. washwashed with acetone