HRID258354

反应详情

EQUATION

反应方程式

HRID 258354 的结构方程式

PROCEDURE

实验过程

1-Amino-2-(3'-amino-4'-sulfophenoxy)-4-(4'-sulfophenylthio)anthraquinone (6 parts) and cyanuric chloride (1.8 parts) were subjected a to condensation reaction in an aqueous medium in a conventional manner, followed by a condensation reaction with 3-aminobenzenesulfonic acid (1.7 parts) at 20° to 40° C. under a weak acid condition. Thereafter, salting out of the reaction mixture with sodium chloride gave an anthraquinone compound of the following formula (free acid form). ##STR215##

WORKUP

后处理

  1. customto condensation reaction in an aqueous medium in a conventional manner