Triethylamine → HCID 3120174, compound

HRID 267886Notes

Reaction equation

HRID 267886 reaction equation
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH2:8])=[CH:5][CH:4]=1.[C:11]12([C:21](Cl)=[O:22])[CH2:20][CH:15]3[CH2:16][CH:17]([CH2:19][CH:13]([CH2:14]3)[CH2:12]1)[CH2:18]2.C(N(CC)CC)C>C(Cl)(Cl)Cl>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:8][C:21]([C:11]23[CH2:20][CH:15]4[CH2:14][CH:13]([CH2:19][CH:17]([CH2:16]4)[CH2:18]2)[CH2:12]3)=[O:22])=[CH:5][CH:4]=1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 754524-MethoxybenzylamineHCID 989151-Adamantanecarbonyl chloride

Product 1

HCID 3120174HCID 3120174, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Subject 4.0 g. (29.0 mmoles) of p-methoxy-benzylamine, 5.7 g. (29.0 mmoles) of adamantane carboxylic acid chloride and 10 ml. of triethylamine to the process of Example 11. Crystallize the residue obtained thereby from chloroform to obtain the product of this Example, m.p. 91°-94°C.

Workup

  1. customCrystallize the residue
  2. customobtained

Sources & evidence

ORD record
ord-f01fdefbabc3431cb3c24e8c90405f33
Source dataset
uspto-grants-1976_03
Patent number
US03944675

Reaction notes

Loading…