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HRID273909

反应详情

EQUATION

反应方程式

HRID 273909 的结构方程式

REACTANTS

反应物

3
结构：Nc1cccc2c1C(=O)c1ccccc1C2=O
HCID6710

1-Aminoanthraquinone

C14H9NO2

结构：O=C1c2ccccc2C(=O)c2ccccc21
HCID6780

Anthraquinone

C14H8O2

结构：O=S(=O)(O)O.O=S(=O)=O
HCID24681

未命名化合物

PRODUCTS

生成物

1
结构：O=C1c2ccccc2C(=O)c2c1cccc2S(=O)(=O)O
HCID6713

1-Anthracenesulfonic acid, 9,10-dihydro-9,10-dioxo-

C14H8O5S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=S(=O)([O-])[O-].[Hg+2]
催化剂HCID24544

Mercuric sulfate

HgO4S

PROCEDURE

实验过程

GB-A-1 370 413 discloses a two-step synthesis of 1-aminoanthraquinone, in which anthraquinone is sulfonated with oleum in the presence of mercury sulfate to give anthraquinone-1-sulfonic acid and this is reacted in a second step with ammonia to give 1-aminoanthraquinone.