反应详情

温度

130 °C

88.2 parts of triphenylphosphine was dissolved in 240 parts of xylene and 51.3 parts of cinnamyl chloride was added thereto. The mixture was heated at 130° C. for 4 hr. After the mixture was cooled to 30° C., the resulting colorless crystals were collected by filtration and washed with toluene to obtain 117.4 parts of cinnamyltriphenylphosphonium chloride (compound No. 15).

1. additionwas added
2. temperatureAfter the mixture was cooled to 30° C.
3. filtrationthe resulting colorless crystals were collected by filtration
4. washwashed with toluene