Azobisisobutyronitrile → Styrene octene
Reaction equation
O1[CH:3]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2]1.N(C(C)(C)C#N)=NC(C)(C)C#N>C=CCCCCCC.C=CC1C=CC=CC=1>[CH2:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH2:2]=[CH:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]Participants
5
Reactant 2
Product 1
Reagents, catalysts & solvents 2
Conditions
- Temperature
- 130 °C
Procedure
The epoxyoctane hydrophobic dense star polymer described in Example 10 (0.1 g) was dissolved in a mixture of 1 g of octene and 19 g of styrene. Azobisisobutyronitrile (0.15 g) was added and the resulting solution was heated at 100° C. for 0.5 day and 130° C. for 1 day to give a solid polymer.
Workup
- customto give a solid polymer
Sources & evidence
- ORD record
- ord-80b85be3feb64a0a8bdcd101aab0a634
- Source dataset
- uspto-grants-1995_02
- Patent number
- US05393797
Reaction notes
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