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HRID277634

反应详情

EQUATION

反应方程式

HRID 277634 的结构方程式

REACTANTS

反应物

5
结构：ClCC1CO1
HCID7835

Epichlorohydrin

C3H5ClO

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COc1ccc(N2CCNCC2)cc1OC.Cl.Cl
HCID22625407

1-(3,4-Dimethoxyphenyl)piperazine--hydrogen chloride (1/2)

C12H20Cl2N2O2

结构：Cc1cc(OC(=O)c2ccccc2)c2ccccc2c1O
HCID22625409

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(N2CCN(CC(O)COc3c(C)cc(O)c4ccccc34)CC2)cc1OC
HCID22625385

未命名化合物

收率 8.8%

PROCEDURE

实验过程

Using 2.8 g (0.01 mol) of 4-benzoyloxy-2-methylnaphthol, 1.4 g (0.01 mol) of anhydrous potassium carbonate, 4.6 g (0.05 mol) of chloromethyloxirane, 2.9 g (0.01 mol) of 1-(3,4-dimethoxyphenyl)piperazine dihydrochloride and 2.0 g (0.02 mol) of triethylamine, reaction was carried out as in Examples 3 and 4 to give 0.4 g of white crystals, m.p. 180-182° C. (decomp.).