HRID277887
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 0 °C
PROCEDURE
实验过程
HCl gas was passed through a solution of 5-2 (1.3 g, 3.9 mmol) in EtOAc (25 mL) at 0° C. for 3 min. After stirring at 0° C. for an additional 2 hrs, the reaction mixture was concentrated to give 5-3 as a solid.
WORKUP
后处理
- concentrationthe reaction mixture was concentrated