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HRID325274

反应详情

EQUATION

反应方程式

HRID 325274 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：CC(=O)[O-].CC(=O)[O-].[Mg+2]
HCID8896

Magnesium acetate

C4H6MgO4

结构：CC(=O)CC(=O)N[C@@H](CC(=O)O)C(=O)O
HCID13334672

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)CC(=O)N[C@H]1CC(=O)OC1=O
HCID13334674

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

CONDITIONS

反应条件

温度
55 °C

PROCEDURE

实验过程

21.72 parts of N-acetoacetyl-L-aspartic acid, 0.14 parts of magnesium acetate, and 9.5 parts by volume of acetic anhydride were mixed with 200 parts by volume of ethyl acetate and heated at 55±2° C. under argon for 24 hours.