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HRID332167

反应详情

EQUATION

反应方程式

HRID 332167 的结构方程式

REACTANTS

反应物

3
结构：BrCc1ccccc1
HCID7498

alpha-Bromotoluene

C7H7Br

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：Nc1cc(Cl)ccc1S
HCID12000

2-Amino-4-chlorobenzenethiol

C6H6ClNS

PRODUCTS

生成物

1
结构：Nc1cc(Cl)ccc1SCc1ccccc1
HCID12618210

2-(Benzylsulfanyl)-5-chloroaniline

C13H12ClNS

收率 112.3%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Following General Procedure A, the title compound (819 mg, 100%) was prepared from 2-amino-4-chlorobenzenethiol (700 mg, 4.39 mmol), (bromomethyl)benzene (560 mg, 2.92 mmol), K2CO3 (2.0 g, 14.62 mmol) in DMF (20 ml).