HRID355036

反应详情

EQUATION

反应方程式

HRID 355036 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The product is produced as described in example 1 from 3 g. of NaH (80% suspension in mineral oil), 17 g. of 5-chloro-benzoxazolin-2-one (produced in usual manners by subjecting 2-amino-4-chloro-phenol-hydrochloride to reaction with phosgene), 200 cc. of DMF, 23.7 g. of 8-bromo-caprylic acid methyl ester and 3 g. of NaJ.

WORKUP

后处理

  1. customThe product is produced