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HRID355038

反应详情

EQUATION

反应方程式

HRID 355038 的结构方程式

REACTANTS

反应物

3
结构：O=c1[nH]c2ccccc2[nH]1
HCID11985

Benzimidazolinone

C7H6N2O

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：COC(=O)CCCCCCCBr
HCID11107373

Methyl 8-bromooctanoate

C9H17BrO2

PRODUCTS

生成物

1
结构：COC(=O)CCCCCCCn1c(=O)[nH]c2ccccc21
HCID12961171

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The product is produced as described in example 1 from 2.8 g. of NaH (80% suspension in mineral oil), 25 g. of benzimidazolin-2-one, 180 cc. of DMF, 22.1 g. of 8-bromocaprylic acid methyl ester and 2.8 g. of NaJ. Eluant in chromatographic purification: chloroform/methanol.

WORKUP

后处理

  1. customThe product is produced
  2. customEluant in chromatographic purification