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HRID355045

反应详情

EQUATION

反应方程式

HRID 355045 的结构方程式

REACTANTS

反应物

3
结构：ClCc1ccccc1Cl
HCID11906

2-Chlorobenzyl chloride

C7H6Cl2

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：COC(=O)CCCCCCCn1c(=O)[nH]c2ccccc21
HCID12961171

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)CCCCCCCn1c(=O)n(Cc2ccccc2Cl)c2ccccc21
HCID54064410

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The product is produced as described in example 1 from 0.72 g. of NaH (80% suspension in mineral oil), 7 g. of 8-(2-oxobenzimidazolin-1-yl)-caprylic acid methyl ester, 100 cc. of DMF, 3.9 g. of 2-chlorobenzylchloride and 0.72 g. of NaJ. Eluant of chromatographic purification: hexane/ethylacetate.

WORKUP

后处理

  1. customThe product is produced
  2. customEluant of chromatographic purification