1-Octene → Biphenyl

HRID 357943Notes

Reaction equation

HRID 357943 reaction equation
C=CCCCCCC.Ic1ccccc1>FC(F)(F)c1ccc(N2CP(C3CCCCC3)CN(c3ccc(C(F)(F)F)cc3)CP(C3CCCCC3)C2)cc1.CCN(CC)CC.Cc1ccccc1.O=C(/C=C/c1ccccc1)/C=C/c1ccccc1.O=C(/C=C/c1ccccc1)/C=C/c1ccccc1.O=C(/C=C/c1ccccc1)/C=C/c1ccccc1.[Pd].[Pd]>c1ccc(-c2ccccc2)cc1.COc1cc(OC)cc(OC)c1.CCCCCC/C=C/c1ccccc1.C=C(CCCCCC)c1ccccc1

Participants

10

Reactant 2

HCID 81251-OcteneHCID 11575Iodobenzene

Product 4

HCID 7095BiphenylHCID 693011,3,5-TrimethoxybenzeneHCID 5369452HCID 5369452, compoundHCID 12396457(Oct-1-en-2-yl)benzene

Reagents, catalysts & solvents 4

HCID 8471TriethylamineReagentHCID 177746363PC2yNArCF32CatalystHCID 1140TolueneSolventHCID 9811564Bis(dibenzylideneacetone)palladiumOther

Conditions

Temperature
85 °C

Workup

  1. additionKeep Filtrate

Sources & evidence

ORD record
ord-3b87e24c689e4fcda664ebf3e111dcd6
Source dataset
1-octene Mizoroki-Heck

Reaction notes

Loading…