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HRID361799

反应详情

EQUATION

反应方程式

HRID 361799 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)c1ccc[nH]1
HCID12473

2-Pyrrolecarboxylic acid

C5H5NO2

结构：O=C(n1ccnc1)n1ccnc1
HCID68263

1,1'-Carbonylbis(1H-imidazole)

C7H6N4O

结构：CCN(c1ncccc1C=C(C)C)C1CCN(Cc2ccccc2)CC1
HCID10665494

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1cccnc1N(C)C1CCN(C(=O)c2ccc[nH]2)CC1
HCID15392051

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[OH-].[OH-].[Pd+2]
催化剂HCID9942167

Palladium hydroxide

H2O2Pd

PROCEDURE

实验过程

Following the general procedure of EXAMPLE 20 and making non-critical variations but starting with 1-benzyl-4-(N-methyl-N-(3-(1-propenyl)-2-pyridinyl)amino)piperidine (XXII, EXAMPLE 14, 0.46 g, mmol), Pearlman's catalyst (0.1 g), CDI (0.46 g, 2.85 mmol) and pyrrole-2-carboxylic acid (0.32 g, 2.85 mmol), the title compound is obtained, mp 88°-90°.