HRID384586

反应详情

EQUATION

反应方程式

HRID 384586 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a mixture of 2.22 g (29.6 mmol) of 3-amino-1-propanol in 20 ml of 1,2-dimethoxyethane and 40 ml of 2-propanol is added a solution of 11.57 g (41.3 mmol) of the compound of Example 1A in 20 ml of 1,2-dimethoxyethane. The mixture is heated at reflux overnight. Solvent is evaporated to afford a mixture of the title compounds.

WORKUP

后处理

  1. temperatureThe mixture is heated
  2. temperatureat reflux overnight
  3. customSolvent is evaporated
  4. customto afford