HRID403996

反应详情

EQUATION

反应方程式

HRID 403996 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The compound of example 403 (80 mg, 0.160 mmol) was taken in THF (4 mL) and MeOH (1 mL) and to this reaction mixture, 1N LiOH (33.59 mg, 0.800 mmol) was added and stirred at room temperature for 2-3 h. After completion of the reaction, the solvent was evaporated and the residue obtained was dissolved in water and acidified with 1 N HCl to obtain the title compound, which was filtered and dried.

WORKUP

后处理

  1. customAfter completion of the reaction
  2. customthe solvent was evaporated
  3. customthe residue obtained