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HRID410758

反应详情

EQUATION

反应方程式

HRID 410758 的结构方程式

REACTANTS

反应物

3
结构：CN
HCID6329

Methylamine

CH5N

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CNc1cc(C(=O)O)ccc1[N+](=O)[O-]
HCID22184623

3-(Methylamino)-4-nitrobenzoic acid

C8H8N2O4

PRODUCTS

生成物

1
结构：CNC(=O)c1ccc([N+](=O)[O-])c(NC)c1
HCID60144426

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[N-]=[N+]=NP(=O)(c1ccccc1)c1ccccc1
溶剂HCID199401

Phosphinic azide, diphenyl-

C12H10N3OP

PROCEDURE

实验过程

N-Methyl-3-methylamino-4-nitro-benzamide (407 mg) was prepared by following General Procedure N starting from 3-methylamino-4-nitro-benzoic acid (500 mg), DPPA (550 uL), DIEA (445 uL), and methylamine (2 M in THF, 2.55 mL).