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HRID410762

反应详情

EQUATION

反应方程式

HRID 410762 的结构方程式

REACTANTS

反应物

4
结构：COCCN
HCID8018

2-Methoxyethylamine

C3H9NO

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID2733084

Methanaminium, N-[(1H-benzotriazol-1-yloxy)(dimethylamino)methylene]-N-methyl-, hexafluorophosphate(1-) (1:1)

C11H16F6N5OP

结构：CNc1cc(F)c(C(=O)O)cc1[N+](=O)[O-]
HCID59529834

未命名化合物

PRODUCTS

生成物

1
结构：CNc1cc(F)c(C(=O)NCCOC)cc1[N+](=O)[O-]
HCID67335417

未命名化合物

PROCEDURE

实验过程

2-Fluoro-N-(2-methoxy-ethyl)-4-methylamino-5-nitro-benzamide was prepared by following General Procedure F starting from 2-fluoro-4-methylamino-5-nitro-benzoic acid (75 mg), HBTU (159 mg), DIEA (92 uL), and 2-methoxyethylamine (26 mg). The crude product was used directly in the next step without further purification.

WORKUP

后处理

  1. customThe crude product was used directly in the next step without further purification