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HRID410902

反应详情

EQUATION

反应方程式

HRID 410902 的结构方程式

REACTANTS

反应物

2
结构：COCCN
HCID8018

2-Methoxyethylamine

C3H9NO

结构：COC(=O)c1ccc(Cl)c([N+](=O)[O-])c1
HCID735797

Methyl 4-chloro-3-nitrobenzoate

C8H6ClNO4

PRODUCTS

生成物

1
结构：COCCNc1ccc(C(=O)OC)cc1[N+](=O)[O-]
HCID67335214

未命名化合物

收率 81.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

4-(2-Methoxy-ethylamino)-3-nitro-benzoic acid methyl ester (960.0 mg) was prepared by following General Procedure A starting from methyl 4-chloro-3-nitrobenzoate (1.0 g) and 2-methoxy-ethylamine (413.0 mg) in DMF (10.0 mL). The crude product was used in the next step without further purification.

WORKUP

后处理

  1. customThe crude product was used in the next step without further purification