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HRID420879

反应详情

EQUATION

反应方程式

HRID 420879 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：Nc1ccnc(Cl)c1N
HCID285736

2-chloropyridine-3,4-diamine

C5H6ClN3

PRODUCTS

生成物

1
结构：CC(=O)Nc1c(N)ccnc1Cl
HCID45119288

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

1.1 A solution of 10.0 g of 3,4-diamino-2-chloropyridine and 6.62 ml of acetic anhydride in 100 ml of THF is stirred at room temperature for 16 hours. The product is separated off and dried, giving 7.3 g of N-(4-amino-2-chloropyridin-3-yl)acetamide (“1”).

WORKUP

后处理

  1. customThe product is separated off
  2. customdried