HRID424309

反应详情

EQUATION

反应方程式

HRID 424309 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Following the same preparation procedure of Example 2, the reaction was carried out with 4-hydroxy bromophenol (4 g), 2-hydroxypropyl 2-methylacrylate (3.33 g), triphenyl phosphine (6.06 g) and DIAD (4.69 g) in 50 ml of THF to give after chromatography purification pure 2-(4-bromophenoxy)propyl 2-methylacrylate as pale yellow oil.

WORKUP

后处理

  1. customthe same preparation procedure of Example 2
  2. customto give
  3. customafter chromatography purification pure 2-(4-bromophenoxy)propyl 2-methylacrylate as pale yellow oil