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HRID429343

反应详情

EQUATION

反应方程式

HRID 429343 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CN1CCCC1CCCl
HCID285093

2-(2-Chloroethyl)-1-methylpyrrolidine

C7H14ClN

结构：COc1ccc(S)cc1F
HCID2759007

3-Fluoro-4-methoxythiophenol

C7H7FOS

PRODUCTS

生成物

1
结构：Cc1ccc(SCCC2CCCN2C)cc1F
HCID18355468

未命名化合物

收率 74.2%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

2-(2-Chloroethyl)-1-methylpyrrolidine (1.4 g, 9.48 mmole), 3-fluoro-4-methyoxythiophenol (1.5 g, 9.48 mmole), potassium carbonate (13.1 g, 94.8 mmole) and DMF (20 mL) were combined, yielding 1.90 g (7.03 mmole, 74%) of the desired compound.