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HRID458872

反应详情

EQUATION

反应方程式

HRID 458872 的结构方程式

REACTANTS

反应物

4
结构：c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID11776

Triphenylphosphine

C18H15P

结构：CCOC(=O)N=NC(=O)OCC
HCID220568

Diethyl azodicarboxylate

C6H10N2O4

结构：O=C1NC(=O)C23CCCc4cccc(c42)C(=O)C13
HCID598548

3a,4,5,6-Tetrahydrosuccinimido[3,4-b]acenaphthen-10-one

C14H11NO3

结构：O=C(C=Cc1cccnc1)NCCCCO
HCID53817888

未命名化合物

PRODUCTS

生成物

1
结构：O=C(C=Cc1cccnc1)NCCCCN1C(=O)C2CC3=C4C(=CCC3)C=CC(=O)C42C1=O
HCID68504233

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Batch size: 4.4 g (20.0 mmol) N-(4-hydroxy-butyl)-3-pyridin-3-yl-acrylamide, 5.2 g (19.8 mmol) triphenylphosphine, 4.8 g (19.9 mmol) 7,8-dihydroacenaphthen-2(6H)-on-1,8a-dicarboximide and 3.5 g (20.0 mmol) azodicarboxylic acid diethyl ester in 65 ml THF.