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HRID463024

反应详情

EQUATION

反应方程式

HRID 463024 的结构方程式

REACTANTS

反应物

4
结构：O=C1c2ccccc2C(=O)N1CCCBr
HCID21611

N-3-Bromopropylphthalimide

C11H10BrNO2

结构：NN.O
HCID24654

Hydrazine hydrate (1:1)

H6N2O

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

2 次

结构：O=C(c1ccccc1)c1ccccc1Nc1ncccc1[N+](=O)[O-]
HCID13388384

{2-[(3-Nitropyridin-2-yl)amino]phenyl}(phenyl)methanone

C18H13N3O3

PRODUCTS

生成物

1
结构：NCCCN(c1ccccc1C(=O)c1ccccc1)c1ncccc1[N+](=O)[O-]
HCID53831951

{2-[(3-Aminopropyl)(3-nitropyridin-2-yl)amino]phenyl}(phenyl)methanone

C21H20N4O3

PROCEDURE

实验过程

[2-[(3-Nitro-2-pyridinyl)amino]phenyl]phenylmethanone is reacted with (a) sodium hydride in solvent followed by N-(3-bromopropyl)phthalimide. The product of (a) is reacted with alcholic hydrazine hydrate and acid to give the title compound.