HRID469138
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of Fmoc-Xaa-OH (2 eq.), TBTU (2 eq.), HOBt (hydroxybenzotriazole) (2 eq.), DIEA (5.2 eq.) in NMP was added to the resin-bound free amine peptide and shaken for 60 min at room temperature and washed with NMP (5×).
WORKUP
后处理
- washwashed with NMP (5×)