HRID513766
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
In a similar fashion using route 51 general procedure 118, 12-chloro-9-fluoro-5H-6-thia-4,5-diaza-chrysene 6,6-dioxide 503 (200 mg, 0.6 mmol), piperidine (195 mg, 2.3 mmol) and NMP (2 ml) gave title compound (50 mg, 21%) after purification by column chromatography using DCM/MeOH (99.5:0.5) as the eluent.