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HRID52753

反应详情

EQUATION

反应方程式

HRID 52753 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1cccc([N+](=O)[O-])c1
HCID7449

3-Nitrobenzaldehyde

C7H5NO3

结构：C1CCNCC1
HCID8082

Piperidine

C5H11N

结构：CC(C)(C)c1cccc(C(C)(C)C)c1O
HCID31405

2,6-Di-tert-butylphenol

C14H22O

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc(C(c2cccc([N+](=O)[O-])c2)N2CCCCC2)cc(C(C)(C)C)c1O
HCID19963870

未命名化合物

收率 60%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1C
溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

Using the same procedure described in Example 4, 30.2 g (0.2 mol) of 3-nitro-benzaldehyde, 37.4 g (0.44 mol) of piperidine and 39.2 g (0.19 mol) of 2,6-di-tert-butyl-phenol are allowed to react in xylene to give 48.4 g of the title compound as yellow crystals, melting at 157° C.