Palmitic Acid → HCID 178484397, compound

HRID 579847Notes

Reaction equation

HRID 579847 reaction equation
C(O)(=O)CCCCCCCCCCCCCCC.[O:19]=[C:20]1[O:26][C@H:25]([C@H:27]([CH2:29][OH:30])[OH:28])[C:23]([OH:24])=[C:21]1[OH:22].[CH3:31][NH:32][C:33]([NH:38][CH2:39][CH2:40][S:41][CH2:42][C:43]1[O:47][C:46]([CH2:48][N:49]([CH3:51])[CH3:50])=[CH:45][CH:44]=1)=[CH:34][N+:35]([O-:37])=[O:36]>ClCCl>[CH3:31][NH:32][C:33]([NH:38][CH2:39][CH2:40][S:41][CH2:42][C:43]1[O:47][C:46]([CH2:48][N:49]([CH3:50])[CH3:51])=[CH:45][CH:44]=1)=[CH:34][N+:35]([O-:37])=[O:36].[O:19]=[C:20]1[O:26][C@H:25]([C@H:27]([CH2:29][OH:30])[OH:28])[C:23]([O-:24])=[C:21]1[OH:22]

Participants

5

Reactant 3

HCID 985Palmitic AcidHCID 5039RanisenHCID 54670067L-Ascorbic Acid

Product 1

HCID 178484397HCID 178484397, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

2.45 g of palmitic acid were dissolved in 10 ml of dichloromethane. Thereafter, 0.88 g (0.5 cmole) of ascorbic acid and 1.57 g (0.5 cmole) of ranitidine were added. The mixture was stirred for 3 hours at room temperature, was filtered and washed with the same liquors. Dry weight: 3.56 g. This solid is unaltered by ambient conditions.

Workup

  1. filtrationwas filtered
  2. washwashed with the same liquors
  3. customDry weight

Sources & evidence

ORD record
ord-47a3160ae6424f6cbcc9732d412eb9fe
Source dataset
uspto-grants-1988_06
Patent number
US04749790

Reaction notes

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