HRID605398

反应详情

EQUATION

反应方程式

HRID 605398 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The product of Example 438B (0.40 g, 0.96 mmol) and 20% palladium hydroxide on carbon (0.21 g) in a ethyl acetate (10 mL) and methanol (1 mL) was stirred under a an atmosphere of hydrogen for 0.5 hours. The reaction was filtered through a bed of celite and concentrate to give the title product (0.256 g).

WORKUP

后处理

  1. filtrationThe reaction was filtered through a bed of celite
  2. concentrationconcentrate