反应详情

温度

60 °C

A mixture of 3-hydroxy-4-nitrobenzaldehyde (51.3 g), iodomethane (38.3 ml) and K2CO3 (85 g) in DMF (250 ml) was stirred at 60° C. for 1 h. The reaction mixture was cooled to room temperature and poured into water (600 ml). The solids were collected by filtration and dried in vacuo (50° C.).

1. temperatureThe reaction mixture was cooled to room temperature
2. filtrationThe solids were collected by filtration
3. customdried in vacuo (50° C.)