反应详情

A mixture of 7-fluoro-2(1H)-quinoxalinone (3.84 g, 23 mmol), allyl iodide (2.39 mL, 25.5 mmol) and potassium carbonate (9.56 g, 69.3 mmol) in dimethylformamide (60 mL) was stirred at room temp. for 3 h., then evaporated. The residue was dissolved in dichloromethane/water and the phases were separated. The aqueous phase was extracted (3×) with dichloromethane and the organic fractions were dried and evaporated.

1. customevaporated
2. dissolutionThe residue was dissolved in dichloromethane/water
3. customthe phases were separated
4. extractionThe aqueous phase was extracted (3×) with dichloromethane
5. customthe organic fractions were dried
6. customevaporated