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HRID657168

反应详情

EQUATION

反应方程式

HRID 657168 的结构方程式

REACTANTS

反应物

3
结构：CCOC=O
HCID8025

Ethyl formate

C3H6O2

结构：CCOC(=O)CCCC(=O)OCC
HCID13163

Diethyl glutarate

C9H16O4

结构：[Na]
HCID5360545

Sodium

Na

PRODUCTS

生成物

1
结构：CCOC(=O)CCC(C=O)C(=O)OCC.[Na]
HCID86635375

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

Prepared from diethyl glutarate and ethyl formate in the presence of sodium metal in diethyl ether according to the literature procedure (J. Bigs, P. Sykes, J. Chemical Society (1959), 1849-55). Obtained solid (28 g; 45%). LCMS (ES+) m/z 238 (MH+).

WORKUP

后处理

  1. customObtained solid (28 g; 45%)