HRID660700
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of 1-(3-benzyloxy-4-nitrophenyl)-2-methylpentan-3-one (450 mg) and Pt/C (22 mg) in EtOAc (15 mL) is hydrogenated at 1 atm for 18 h. The catalyst is filtered and the filtrate evaporated to give the title compound which is used directly in the next step.
WORKUP
后处理
- filtrationThe catalyst is filtered
- customthe filtrate evaporated