huagongshe.com
HRID69924

反应详情

EQUATION

反应方程式

HRID 69924 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=[N+]([O-])c1cnccc1Cl
HCID2735781

4-Chloro-3-nitropyridine

C5H3ClN2O2

结构：CC1(O)CCCNC1
HCID22496626

3-Methylpiperidin-3-ol

C6H13NO

PRODUCTS

生成物

1
结构：CC1(O)CCCN(c2ccncc2[N+](=O)[O-])C1
HCID69041542

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Method 1 of Example 1 was followed using 1 equivalent each of 4-chloro-3-nitropyridine, 3-methylpiperidin-3-ol and triethyl amine in DMF yielding 3-methyl-1-(3-nitropyridin-4-yl)piperidin-3-ol. LCMS (m/z): 238.1 (MH+); LC Rt=1.39 min.