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HRID70457

反应详情

EQUATION

反应方程式

HRID 70457 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COC(=O)c1ccc(CBr)cc1
HCID256687

Methyl 4-(bromomethyl)benzoate

C9H9BrO2

结构：Nc1cc(F)ccc1S
HCID11105480

2-amino-4-fluorobenzene-1-thiol

C6H6FNS

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(CSc2ccc(F)cc2N)cc1
HCID43304285

未命名化合物

收率 94%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Following General Procedure A, the title compound (873 mg, 94%) was prepared from 2-amino-4-fluorobenzenethiol (456 mg, 3.19 mmol) and methyl 4-(bromomethyl)benzoate (731 mg, 3.19 mmol), K2CO3 (1.32 g, 9.58 mmol) in DMF (20 ml).