Diethylamine → HCID 23112247, compound

HRID 731947Notes

Reaction equation

HRID 731947 reaction equation
[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][O:11][CH:10]([C:14]([OH:16])=O)[CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH2:17]([NH:19][CH2:20][CH3:21])[CH3:18].C(N=C=NCCCN(C)C)C>CN(C=O)C>[CH2:17]([N:19]([CH2:20][CH3:21])[C:14]([CH:10]1[O:11][CH2:12][CH2:13][N:8]([C:6]([O:5][C:1]([CH3:2])([CH3:3])[CH3:4])=[O:7])[CH2:9]1)=[O:16])[CH3:18]

Participants

5

Reactant 3

HCID 8021DiethylamineHCID 159081-Ethyl-3-(3'-dimethylaminopropyl)carbodiimideHCID 27559654-((Tert-butoxy)carbonyl)morpholine-2-carboxylic acid

Product 1

HCID 23112247HCID 23112247, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

4-(t-Butoxycarbonyl)morpholine-2-carboxylic acid and diethylamine were dissolved in DMF, 1-ethyl-3-(3′-dimethylaminopropyl)carbodiimide was added thereto at room temperature, and the whole was stirred to obtain t-butyl 2-[(diethylamino)carbonyl]morpholine-4-carboxylate.

Sources & evidence

ORD record
ord-adfc971299f1469a855e6ef45152b363
Source dataset
uspto-grants-2009_09
Patent number
US07585878B2

Reaction notes

Loading…