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HRID743009

反应详情

EQUATION

反应方程式

HRID 743009 的结构方程式

REACTANTS

反应物

3
结构：CCCCN(CCCC)CCCC
HCID7622

Tributylamine

C12H27N

结构：C=Cc1ccc(S(=O)(=O)Nc2ncccc2C)cc1
HCID19423365

未命名化合物

结构：CC(C)COC(=O)c1cc(I)ccc1O
HCID19423370

2-Methylpropyl 2-hydroxy-5-iodobenzoate

C11H13IO3

PRODUCTS

生成物

1
结构：Cc1cccnc1NS(=O)(=O)c1ccc(C=Cc2ccc(O)c(C(=O)OCC(C)C)c2)cc1
HCID54356729

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CC(=O)[O-].CC(=O)[O-].[Pd+2]
催化剂HCID167845

Diacetatopalladium

C4H6O4Pd

结构：CC(=O)N(C)C
溶剂HCID31374

Dimethylacetamide

C4H9NO

PROCEDURE

实验过程

Isobutyl 2-hydroxy-5-iodobenzoate (70.2 g, 0.22 mol) and 4-ethenyl-N-(3-methyl-2pyridinyl)benzensulfonamide (54.8 g, 0.20 mol) were suspended in a solution of tributylamine (55.5 g, 0.3 mol) and palladium(II) acetate (0.44 g 0.0022 mol) in dimethylacetamide (200 ml)