Hydrochloric Acid → N-methyl-N-methyloxy-2-benzyloxycarbonylamino-5-hydroxybenzamide

HRID 800466Notes

Reaction equation

HRID 800466 reaction equation
[CH2:1]([c:2]1[cH:3][cH:4][cH:5][cH:6][cH:7]1)[O:8][C:9](=[O:10])[NH:11][c:12]1[c:13]([C:14](=[O:15])[OH:16])[cH:17][c:18]([OH:21])[cH:19][cH:20]1.[CH2:28]([N:29]=[C:30]=[N:31][CH2:32][CH2:33][CH2:34][N:35]([CH3:36])[CH3:37])[CH3:38].[CH3:23][NH:24][O:25][CH3:26].[CH3:39][CH2:40][N:41]([CH2:42][CH3:43])[CH2:44][CH3:45].[ClH:22].[ClH:27]>>[CH2:1]([c:2]1[cH:3][cH:4][cH:5][cH:6][cH:7]1)[O:8][C:9](=[O:10])[NH:11][c:12]1[c:13]([C:14](=[O:16])[N:24]([CH3:23])[O:25][CH3:26])[cH:17][c:18]([OH:21])[cH:19][cH:20]1

Participants

6

Reactant 5

HCID 313Hydrochloric Acid2×HCID 8471TriethylamineHCID 14232N,O-DimethylhydroxylamineHCID 159081-Ethyl-3-(3'-dimethylaminopropyl)carbodiimideHCID 183153542-(((Benzyloxy)carbonyl)amino)-5-hydroxybenzoic acid

Product 1

HCID 18315375N-methyl-N-methyloxy-2-benzyloxycarbonylamino-5-hydroxybenzamide

Sources & evidence

ORD record
ord-9bd0513761ba4fdd9d1cc674c79e5ff8
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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