Sulfuric Acid → Ethyl tetrahydro-4-hydroxy-2H-pyran-4-acetate

HRID 816042Notes

Reaction equation

HRID 816042 reaction equation
[Br:9][CH2:10][C:11](=[O:12])[O:13][CH2:14][CH3:15].[I:8].[O:1]1[CH2:2][CH2:3][C:4](=[O:7])[CH2:5][CH2:6]1.[O:21]1[CH2:22][CH2:23][CH2:24][CH2:25]1.[S:16](=[O:17])(=[O:18])([OH:19])[OH:20].[Zn:26]>>[O:1]1[CH2:2][CH2:3][C:4]([OH:7])([CH2:10][C:11](=[O:12])[O:13][CH2:14][CH3:15])[CH2:5][CH2:6]1

Participants

7

Reactant 6

HCID 1118Sulfuric AcidHCID 7748Ethyl bromoacetateHCID 8028TetrahydrofuranHCID 23994ZincHCID 24841Hydrogen iodideHCID 121599Tetrahydro-4H-pyran-4-one

Product 1

HCID 21936035Ethyl tetrahydro-4-hydroxy-2H-pyran-4-acetate

Sources & evidence

ORD record
ord-c75e31060f3d41719836347a76ac2e64
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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