Ammonium → tert-Butyl 3-azidopiperidine-1-carboxylate

HRID 820189Notes

Reaction equation

HRID 820189 reaction equation
[C:7]([CH3:8])([CH3:9])([CH3:10])[O:11][C:12](=[O:13])[N:14]1[CH2:15][CH:16]([O:20][S:21]([CH3:22])(=[O:23])=[O:24])[CH2:17][CH2:18][CH2:19]1.[Cl-:5].[N-:2]=[N+:3]=[N-:4].[NH4+:6].[Na+:1].[O:25]=[CH:26][N:27]([CH3:28])[CH3:29].[OH2:30]>>[N:2](=[N+:3]=[N-:4])[CH:16]1[CH2:15][N:14]([C:12]([O:11][C:7]([CH3:8])([CH3:9])[CH3:10])=[O:13])[CH2:19][CH2:18][CH2:17]1

Participants

8

Reactant 7

HCID 223AmmoniumHCID 312ChlorideHCID 923Sodium ionHCID 962WaterHCID 6228DimethylformamideHCID 33558AzideHCID 568122N-Boc-3-mesyloxypiperidine

Product 1

HCID 547722tert-Butyl 3-azidopiperidine-1-carboxylate

Sources & evidence

ORD record
ord-4c7b3608bacf499db08547cc6eaf3a12
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

Loading…