Ammonium → Tert-butyl 3-(methanesulfonyloxy)azetidine-1-carboxylate

HRID 822634Notes

Reaction equation

HRID 822634 reaction equation
[CH3:1][CH2:2][N:3]([CH2:4][CH3:5])[CH2:6][CH3:7].[CH3:27][CH2:28][O:29][C:30](=[O:31])[CH3:32].[CH3:8][S:9]([Cl:10])(=[O:11])=[O:12].[CH:33]([Cl:34])([Cl:35])[Cl:36].[Cl-:25].[NH4+:26].[OH:13][CH:14]1[CH2:15][N:16]([C:18](=[O:19])[O:20][C:21]([CH3:22])([CH3:23])[CH3:24])[CH2:17]1>>[CH3:8][S:9](=[O:11])(=[O:12])[O:13][CH:14]1[CH2:15][N:16]([C:18](=[O:19])[O:20][C:21]([CH3:22])([CH3:23])[CH3:24])[CH2:17]1

Participants

8

Reactant 7

HCID 223AmmoniumHCID 312ChlorideHCID 6212ChloroformHCID 8471TriethylamineHCID 8857Ethyl AcetateHCID 31297Methanesulfonyl chlorideHCID 2756801Tert-butyl 3-hydroxyazetidine-1-carboxylate

Product 1

HCID 10753243Tert-butyl 3-(methanesulfonyloxy)azetidine-1-carboxylate

Sources & evidence

ORD record
ord-3ade815517e74f12a721daad53549ac1
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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